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Ge et al. Microstructures 2023;3:2023026  https://dx.doi.org/10.20517/microstructures.2023.13  Page 9 of 10

               therefore, a necessary prerequisite for high-performance BiFeO  crystals and ceramics.
                                                                    3

               DECLARATIONS
               Authors’ contributions
               Performed data acquisition, data analysis, and interpretation and wrote the first draft of the article: Ge W,
               Sanchez AM
               Performed data acquisition (STEM+EELS maps) at SuperSTEM: Ramasse Q
               Provided material, conception and design of the study and interpretation: Alexe M
               Performed data analysis and interpretation and contributed to the development of the article: Beanland R,
               Sanchez AM


               AVAILABILITY OF DATA AND MATERIALS
               The data that support the findings of this study are openly available in WRAP at http://wrap.warwick.ac.uk/
               173964.

               Financial support and sponsorship
               Ge  W.  acknowledges  support  from  the  EPSRC  International  Doctoral  Scholars  grant,  number
               EP/R513374/1.


               Conflicts of interest
               All authors declare that there are no conflicts of interest.

               Ethical approval and consent to participate
               Not applicable.

               Consent for publication
               Not applicable.

               Copyright
               © The Author(s) 2023.

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