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Feng et al. Chem Synth 2023;3:37  https://dx.doi.org/10.20517/cs.2023.26         Page 9 of 16




















































                Figure 6. (A) Schematic illustration of the synthetic procedure for the mPDA/MXene heterostructure. This figure is quoted with
                permission from Li  et al. [59] ; (B) Schematic illustration of the construction of OMCTs. This figure is quoted with permission from Liu
                et al. [62] . mPDA: Mesoporous polydopamine; OMCTs: ordered mesoporous carbon/titanium carbide heterostructures.

               According to the summary above, the multi-templates method is simple and versatile for preparing
               2DMMs. Compared with other synthesis methods, the multi-templates method can effectively design and
               control the mesostructure and 2D morphology of the customized 2DMMs. However, it remains challenging
               to achieve narrow distributions and well-defined dimensions of mesoporous structures in 2DMMs by this
               method.

               SURFACE-LIMITED CO-ASSEMBLY METHOD
               The traditional method of synthesizing mesoporous materials using amphiphilic molecules as structure
               guide agents usually uses substrates such as glass, silicon wafers, and others for solid-liquid interface
               assembly synthesis. The obtained materials have low long-term continuity of pore channels and long mass
               transfer distance and are difficult to fully utilize the active sites in pores, which seriously hinders their
               application.
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